Uhlelo Lokuhlola lwe-LADP-2 lwe-NMR edonswayo
I-Pulsed Fourier iguqulela i-resonance kazibuthe wenuzi isebenzisa insimu ye-RF eshaywayo ukusebenza ohlelweni lwenuzi ukubona ukuphendula kohlelo lwenuzi ku-pulse, futhi isebenzisa ubuchwepheshe obusheshayo be-Fourier transform (FFT) ukuguqula isignali yesizinda yesikhathi ibe yisiginali yesizinda semvamisa, okuyi okulingana nemvamisa eyodwa eqhubekayo yamagagasi e-magnetic resonance spectrometers ajabule ngasikhathi sinye, ngakho-ke isimangaliso se-nuclear magnetic resonance singabonwa ebangeni elikhulu, futhi isinali lizinzile Njengamanje, indlela ye-pulse isetshenziswa kuma-spectrometer amaningi e-NMR, ngenkathi indlela ye-pulse isetshenziswa ku-MRI.
Ukuhlolwa
1. Qonda umbono oyisisekelo womzimba nokulungiswa kohlelo lwe-PNMR. Funda ukuchaza izinto ezihlobene ngokomzimba ku-PNMR usebenzisa imodeli ye-vector yakudala.
2. Funda ukusebenzisa amasiginali we-spin echo (SE) nokubola kokungeniswa kwamahhala (FID) ukukala u-T2(isikhathi sokuphumula se-spin-spin). Hlaziya ithonya le-magnetic field homogeneity kusiginali ye-NMR.
3. Funda ukukala u-T1 (isikhathi sokuphumula se-spin-lattice) usebenzisa ukutakula okuphindayo.
4. Ukuqonda ngokufanele indlela yokuphumula, bheka umphumela we-ion paramagnetic esikhathini sokuphumula kwenuzi.
5. Linganisa u-T2Isixazululo se-copper sulfate ezindaweni ezahlukahlukene. Thola ubudlelwane be-T2 ngokushintsha kokuhlushwa.
6. Linganisa ukufuduka kwamakhemikhali okuhlobene kwesampula.
Imininingwane
Incazelo | Imininingwane |
Ukunikezwa kwamandla kwenkambu yokushintshashintsha kwezwi | umkhawulo wamanje ongu-0.5 A, umthethonqubo we-voltage 0 - 6.00 V |
Ukunikezwa kwamandla kwenkambu efanayo | umkhawulo wamanje ongu-0.5 A, umthethonqubo we-voltage 0 - 6.00 V |
Imvamisa ye-Oscillator | 20 MHz |
Amandla endle kazibuthe | 0.470 T |
Ububanzi bepali kazibuthe | 100 mm |
Magnetic pole ibanga | 20 mm |
Ukufana kwensimu yamagnetic | 20 ppm (10 mm × 10 mm × 10 mm) |
Izinga lokushisa elilawulwayo | 36.500 ° C |
Ukuqina kwensimu yamagnetic | Amahora ama-4 afudumele ukuze azinze, imvamisa ye-Larmor ikhukhuleka ngaphansi kuka-5 Hz ngomzuzu. |
Uhlu Lwezingxenye
Incazelo | Inani | Qaphela |
Ukushisa Okuvamile Unit | 1 | kufaka phakathi uzibuthe nedivayisi yokulawula ukushisa |
I-RF Transmitting Unit | 1 | kufaka phakathi ukunikezwa kwamandla kwenkambu yokushintshashintsha |
Iyunithi Yokwamukela Izimpawu | 1 | kufaka phakathi ukunikezwa kwamandla wensimu ehambelana nokubonisa izinga lokushisa |
Intambo yamandla | 1 | |
Ikhebula elihlukahlukene | 12 | |
Amashubhu wesampula | 10 | |
Incwadi Yokufundisa | 1 |