Uhlelo Lokuhlola lwe-LADP-2 lwe-Pulsed NMR
Izivivinyo
1. Qonda ithiyori yomzimba eyisisekelo kanye nokucushwa kokuhlola kohlelo lwe-PNMR.Funda ukuchaza izenzakalo zomzimba ezihlobene ku-PNMR usebenzisa imodeli ye-vector yakudala.
2. Funda ukusebenzisa amasiginali we-spin echo (SE) kanye nokubola kokungeniswa kwamahhala (FID) ukukala i-T2(isikhathi sokuphumula se-spin-spin).Hlaziya umthelela we-magnetic field homogeneity kusiginali ye-NMR.
3. Funda ukukala i-T1(isikhathi sokuphumula se-spin-lattice) usebenzisa ukubuyisela emuva.
4. Qonda ngendlela efanele indlela yokuphumula, bheka umthelela wama-ion we-paramagnetic ngesikhathi sokuphumula kwe-nuclear.
5. Kala u-T2isisombululo se-copper sulfate ezindaweni ezihlukahlukene.Nquma ubudlelwano bukaT2ngokushintsha kokugxilisa ingqondo.
6. Linganisa ukugudluzwa kwamakhemikhali okuhlobene kwesampula.
Imininingwane
Incazelo | Imininingwane |
Ukunikezwa kwamandla kwenkambu yokushintshashintsha | umkhawulo wamanje ngu-0.5 A, ukulawulwa kwamandla kagesi 0 - 6.00 V |
Ukunikezwa kwamandla kwenkambu ye-homogenous | umkhawulo wamanje ngu-0.5 A, ukulawulwa kwamandla kagesi 0 - 6.00 V |
Imvamisa ye-oscillator | 20 MHz |
Amandla enkundla kazibuthe | 0.470 T |
Ububanzi besigxobo sikazibuthe | 100 mm |
Ibanga le-Magnetic pole | 20 mm |
I-homogeneity yensimu yamagnetic | 20 ppm (10 mm × 10 mm × 10 mm) |
Izinga lokushisa elilawulwayo | 36.500 °C |
Ukuzinza kwenkundla kazibuthe | Amahora angu-4 afudumele ukuze azinziswe, i-Larmor frequency drift ngaphansi kuka-5 Hz ngomzuzu. |
Uhlu Lwezingxenye
Incazelo | Qty | Qaphela |
I-Constant Temperature Unit | 1 | okuhlanganisa uzibuthe kanye nedivayisi yokulawula izinga lokushisa |
I-RF Transmitting Unit | 1 | kufaka phakathi ukunikezwa kwamandla kwenkambu yokushintshashintsha |
Iyunithi Yokwamukela Isignali | 1 | okuhlanganisa ukunikezwa kwamandla kwenkambu efanayo kanye nesibonisi sezinga lokushisa |
Intambo Yamandla | 1 | |
Ikhebula elihlukahlukene | 12 | |
Amashubhu esampula | 10 | |
Incwadi Yokufundisa | 1 |